Systems Drugs Column Conc. (µgmL-1) r2 (b) Standard error of estimate Standard error Intercept Slope LLOD (ngmL-1) LLOQ (ngmL-1) LC 10 MET Supelco 2.5-25 0.998 0.3266 0.1668 -0.0454 14520 0.315 0.95 Purospher 2.5-25 0.999 0.3266 0.1668 -0.0454 17505 0.315 0.96 PIO Supelco 2.5-25 0.999 0.31038 0.1631 -0.9252 12516 2.3 0.7 Purospher 2.5-25 0.999 0.31038 0.1631 -0.9252 13959 2.3 0.7 GLB Supelco 2.5-25 0.998 0.3266 0.1668 -0.0454 13520 0.2 0.59 Purospher 2.5-25 0.999 0.3266 0.1668 -0.0454 17505 0.2 0.58 GMP Supelco 2.5-25 0.999 0.31038 0.1631 -0.9252 11516 0.1 0.32 Purospher 2.5-25 0.999 0.31038 0.1631 -0.9252 13969 0.1 0.32 LC 20 MET Supelco 2.5-25 0.998 0.3266 0.1668 -0.0454 13520 0.317 0.96 Purospher 2.5-25 0.999 0.3266 0.1668 -0.0454 17505 0.317 0.96 PIO Supelco 2.5-25 0.999 0.31038 0.1631 -0.9252 11516 2.3 0.7 Purospher 2.5-25 0.999 0.31038 0.1631 -0.9252 13959 2.3 0.7 GLB Supelco 2.5-25 0.998 0.3266 0.1668 -0.0454 13520 0.19 0.58 Purospher 2.5-25 0.999 0.3266 0.1668 -0.0454 17505 0.19 0.58 GMP Supelco 2.5-25 0.999 0.31038 0.1631 -0.9252 11516 0.1 0.32 Purospher 2.5-25 0.999 0.31038 0.1631 -0.9252 13959 0.1 0.32

Table 2: Regression characteristics.

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