| Type |
Statistical parameter |
Concentration (ng/mL) |
LLOQC
(32.05) |
LQC
(100.80) |
MQC
(5040.00) |
HQC
(8400.00) |
Intraday,
set-1,
N=6 |
Mean |
30.06 |
101.98 |
4879.78 |
8258.0 |
| SD |
2.326 |
3.777 |
245.857 |
241.88 |
| % CV |
7.7 |
3.7 |
5.0 |
2.9 |
| Accuracy |
93.80 |
101.17 |
96.82 |
98.31 |
Intraday,
set-2,
N=6 |
Mean |
32.77 |
104.35 |
4887.30 |
8262.61 |
| SD |
1.242 |
4.094 |
262.359 |
260.361 |
| % CV |
3.8 |
3.9 |
5.37 |
3.15 |
| Accuracy |
102.26 |
103.52 |
96.97 |
98.36 |
Intraday,
set-3,
N=6 |
Mean |
29.54 |
101.49 |
4802.93 |
8046.87 |
| SD |
1.706 |
6.969 |
233.780 |
280.376 |
| % CV |
5.77 |
6.87 |
4.87 |
3.48 |
| Accuracy |
92.17 |
100.68 |
95.30 |
95.80 |
Inter day,
N=18 |
Mean |
30.79 |
102.60 |
4856.67 |
8189.15 |
| SD |
2.242 |
5.006 |
235.873 |
266.434 |
| % CV |
7.28 |
4.88 |
4.86 |
3.25 |
| Accuracy |
96.08 |
101.79 |
96.36 |
97.49 |
|
