Parameter Acceptance criteria Results
System Suitability % RSD Not More Than 15.0% 1.6% to 8.1%
Precision % RSD (six sample preparation) Not More Than 15.0% @ LOQ level – 7.7 to 12.2% and 100% Level 3.2 to 7.6%
Linearity Correlation coefficient Not Less Than 0.995 0.997 to 0.998
Accuracy Percent Recovery 85.0% to 115.0% 90.0 to 107.0%
[Overall recovery form LOQ to 150%]
Robustness and Ruggedness % RSD Not More Than 15.0% 4.1 to 8.1%
[Overall compilation of system suitability]
Table 8: Overall compilation of validation [Results of entire study]