| Laboratory |
A |
B |
C |
D |
E |
F |
G |
H |
I |
J |
K |
L |
| |
LC |
2795 (Waters) |
Acquity UPLC (Waters) |
Acquity UPLC (Waters) |
1200 Series (Agilent) |
Nexera (Shimadzu) |
Alliance 2695 (Waters) |
2795 (Waters) |
Acquity UPLC (Waters) |
1100 Series (Agilent) |
1100 Series (Agilent) |
Acquity UPLC (Waters) |
Prominence (Shimadzu) |
| |
MS/MS |
Quattro Premier XE (Waters) |
TQD (Waters) |
Quattro Premier XE (Waters) |
QTRAP 3200 (ABsciex) |
API 4000 (ABsciex) |
Quattro Micro (Waters) |
Quattro Premier XE (Waters) |
TQD (Waters) |
QTRAP 4000 (ABsciex) |
API 3000 (ABsciex) |
Quattro Premier XE (Waters) |
TSQ Quantum Discovery MAX (Thermofisher) |
| NIV |
Precursor ion (m/z) |
371 [M+CH3COO]- |
| Product ion (m/z)1 |
281 |
281 |
281 |
59 |
281 |
281 |
281 |
311 |
59 |
59 |
281 |
281 |
| DON |
Precursor ion (m/z) |
355 [M+CH3COO]- |
| Product ion (m/z)2 |
59 |
295 |
265 |
295, 59 |
265, 59 |
59 |
265 |
59 |
59 |
59 |
265 |
295 |
| ZEA |
Precursor ion (m/z) |
317 [M-H]- |
| Product ion (m/z)3 |
131 |
131 |
175 |
131 |
175 |
175 |
175 |
131 |
131 |
131 |
175 |
131 |
| T-2 |
Precursor ion (m/z) |
484 [M+NH4]+ |
| Product ion (m/z)4 |
215 |
305 |
305 |
215, 185 |
305 |
305 |
305 |
305 |
215 |
215 |
305 |
305 |
| HT-2 |
Precursor ion (m/z) |
442 [M+NH4]+ |
| Product ion (m/z)5 |
263 |
263 |
263, 215 |
263 |
215 |
263 |
263 |
263 |
263 |
263 |
215 |
263 |
| VEL |
Precursor ion (m/z) |
325 [M+CH3COO]- |
| Product ion (m/z) |
59 |
| Precursor ion (m/z) |
284 [M+NH4]+ |
| Product ion (m/z) |
249, 231 |
| ZAN |
Precursor ion (m/z) |
319 [M-H]- |
| Product ion (m/z) |
205, 275 |
|
| 1In addition to the product ion selected in each laboratory for quantification, any of the other product ions (59, 281, and 311) was used as the qualifier ion properly |
| 2 In addition to the product ion selected in each laboratory for quantification, any of the other product ions (59, 265, and 295) was used as the qualifier ion properly |
| 3 In addition to the product ion selected in each laboratory for quantification, any of the other product ions 131 and 175) was used as the qualifier ion properly |
| 4In addition to the product ion selected in each laboratory for quantification, any of the other product ions (185, 215, and 305) was used as the qualifier ion properly |
| 5In addition to the product ion selected in each laboratory for quantification, any of the other product ions (215 and 263) was used as the qualifier ion properly |
| Table 3: LC-MS/MS instruments and parameters used in each laboratory |
