| GC conditions |
MS conditions |
| Column |
DB-5MS, 60 m × 0.32 mm × 1.0 µm |
Ion source temperature (°C) |
230 |
| Carrier gas |
Helium (>99.999%) |
Quadrupole temperature (°C) |
150 |
| Flow rate (ml/min) |
1.5 |
Interface temperature (°C) |
280 |
| Injector |
Splitless |
Range of mass (amu) |
15-300 |
| Column temperature (°C) |
35 (5min) → 150 (5°C/min) → 220 (15°C/min, 7min) |
Scan rate (s/scan) |
0.2 |
| Inlet temperature (°C) |
100 |
Energy of electron ionization source (eV) |
70 |
