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A “salt-free”, automated purge-and-trap sampling method, with gas chromatographic-mass spectrometric detection for simultaneous detection of 2-methylisoborneol (2-MIB) and geosmin (GSM) was developed. The preliminary procedure involved purging a 25 mL water sample, at 80°C for 11 min, with helium gas, and trapping onto a Tenax sorbent.
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