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Cork wastes and by-products were used as raw materials to access sustainable biopolyols in a fast and clean manner. Contributing for the mitigation of a residue recorded as industrial residues in the European waste catalogue and hazardous waste list reducing, therefore, its environmental impact. Cork powder resulting from the cork industry as a waste and/or by-products with no commercial value was subjected to liquefaction in 2-ethyl hexanol/DEG in the presence of p-toluene sulfuric acid. Microwave radiation was used as the heating source. Pulsed microwaves from 150-300 W power were applied for 5-20 min. This alternative energy source was successfully applied leading to a high conversion of cork powder into liquid biopolyols.
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