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The effects of Ag2O-doping on the physicochemical, surface and catalytic properties FeAlO system with various extent of Fe2O3 loading have been investigated. The dopant concentration was changed between 1.5 and 4.0 mol % Ag2O. Pure and variously doped solids were subjected to heat treatment at 400-800?C. The techniques employed for characterization of catalysts were TG/DTG, XRD, N2-adsorption at ?196?C and the catalytic decomposition of H2O2 at 25-40?C. The obtained results revealed that, the investigated catalysts consisted of nanosized ?-Al2O3 phase.