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A comparative study using direct hydrothermal and indirect fusion methods to produce zeolites from coal fly ash utilizing single-mode microwave energy
Microwave irradiation has shown to accelerate zeolitization from several hours to several minutes. A single-mode laboratory-scale microwave was employed, which enabled control of irradiated power and temperature of the reaction mixture, while the pressure was controlled by affixing a condenser on the 40 mL Teflon reactor vessel with a working volume 20 mL. Design of Experiment was used to compare two methods of converting CFA to zeolite-A, direct hydrothermal method and indirect fusion method. Experiments conducted were two level four factorial designs. |
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