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Understanding the interaction between metal nanostructures and common metal ions is essential for biomedical applications of metal nanostructures including imaging and therapy. A systemic study of the interaction of citratecapped hollow gold nanospheres (HGNs), a unique metal nanostructure that has demonstrated high efficiency for photothermal ablation (PTA) therapy of cancer cells, with common metal ions: Na+, Ca2+, Mg2+, Cu2+, Zn2+, and Al3+ was carried out with the goal to determine how these metal ions may affect the properties and thereby performance of HGNs in biomedical applications. View more..