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Electrohydrodynamic atomization phenomena has increasingly attracted the attention of researchers who are interested in pursuing this promising technique to prepare micro- or nanometer architectures such as fibers and encapsulated particles with a controllable microstructure. There are two main techniques in the electrohydrodynamic atomization processing: electrospraying and electrospinning. Electrospraying can create particles by applying a uniform electrohydrodynamic force to break up liquids into fine jets, and is an emerging method for the rapid and high throughput production of nano-meso scale particles of controlled morphology for controlled release during drug delivery. The morphology and size of electrosprayed polymer nanoparticles is strongly influenced by a host of variables that include processing parameters and the material properties of the solution such as polymer composition, molecular weight, the solvent used for polymer dissolution, and the presence and concentration of other cosolutes.