Journal of Analytical & Bioanalytical Techniques
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A novel zirconia nanoparticles based electrochemical sensor has been developed via drop casting method and the
electrochemical sensor was characterized with scanning electron microscopy (SEM). The electrochemical behaviour of
ethionamide (ETA) at zirconia modified glassy carbon electrodes (GCEs) were investigated by cyclic voltammetry (CV) and
square-wave voltammetry (SWV) and results indicated that the electrode process is diffusion controlled. The decrease of charge
transfer resistance was also analysed by electrochemical impedance spectroscopy. Under the optimal conditions, the peak current
of SWV increased linearly with the ETA concentration in the range from 150 - 650 ng/mL with a limit of detection (LOD) 47.66
ng/mL and its application for the electrochemical detection of ethionamide (ETA) in solubilized system has also been reported.
/GCE; ETA; Voltammetry; Pharmaceutical formulation.
Rajeev Jain completed his B.Sc. and M.Sc. from Meerut University, Meerut (Now C.C.S. University, Meerut) and Ph.D. in Chemistry from the University
of Roorkee (now Indian Institute of Technology, Roorkee), India, in 1978. He is a highly cited researcher in Electroanalytical and Environmental
Engineering Chemistry. He has published over 273 research papers in journals of international repute with high impact factor. He has supervised
over 60 Ph.D. and one D.Sc. student. He is a widely traveled researcher and has worked over on 15 research projects sanctioned by CSIR, UGC,
MOEF, and DRDO etc. His research interests include electroanalytical behaviour of pharmaceuticals, micellar catalysis, electrocatalysed reactions,
method development and validation, environmental engineering chemistry and wastewater treatment.
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